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  • 2021

    7-7

    對(duì)于島津液相色譜柱你還有什么不了解的?

    島津液相色譜柱的系統(tǒng)由儲(chǔ)液器、泵、進(jìn)樣器、色譜柱、檢測(cè)器、記錄儀等幾部分組成。儲(chǔ)液器中的流動(dòng)相被高壓泵打入系統(tǒng),樣品溶液經(jīng)進(jìn)樣器進(jìn)入流動(dòng)相,被流動(dòng)相載入色譜柱(固定相)內(nèi),由于樣品溶液中的各組分在兩相中具有不同的分配系數(shù),在兩相中作相對(duì)運(yùn)動(dòng)...

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  • 2021

    7-5

    液相色譜柱的組成結(jié)構(gòu)說(shuō)明

    液相色譜柱是液相色譜分離能力的核心部分,由柱管、壓帽、卡套(密封環(huán))、篩板(濾片)、接頭、螺絲(封頭)與柱填料等組成。1、柱管:多用不銹鋼制成,若果使用時(shí)柱壓不高于70kg/cm2時(shí),也可采用厚壁玻璃或石英管,管內(nèi)壁要求有很高的光潔度。用于...

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  • 2021

    7-5

    Wondasil色譜柱的維護(hù)保養(yǎng)

    Wondasil色譜柱功能特點(diǎn):1.高惰性,無(wú)論酸性化合物還是堿性化合物,都能得到尖銳的峰型。由于機(jī)體硅膠純度高,金屬配位性化合物也能分析。PH10即使是強(qiáng)堿性溶離液下也能維持高性能。2.如果樣品極性太強(qiáng),或酸性太強(qiáng);可以選擇CN,NH2,...

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  • 2021

    6-29

    在哪些情況下要使用到GL Sciences色譜柱

    GLSciences色譜柱的通常有較高的物理穩(wěn)定性和效能,但不能在堿性的條件下使用,殘留的硅烷醇基會(huì)吸附有機(jī)堿。均采用新型的硅膠,其表面經(jīng)過(guò)改良,能準(zhǔn)確的控制硅膠的特性,不僅囊括傳統(tǒng)InertSil的好處(低運(yùn)作背壓、高惰性,高效能,能應(yīng)用...

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  • 2021

    6-28

    氣相色譜柱進(jìn)樣量和氣化溫度的選擇

    氣相色譜柱利用色譜柱先將混合物分離,然后利用檢測(cè)器依次檢測(cè)已分離出來(lái)的組分。在石油、化工、生物化學(xué)、食品工業(yè)、環(huán)保等方面應(yīng)用很廣。氣相色譜操作條件的選擇,常常決定是否能夠達(dá)到分離的目的。下面主要介紹進(jìn)樣量和氣化溫度的選擇:1、進(jìn)樣量的選擇進(jìn)...

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  • 2021

    6-24

    影響尺寸排阻色譜法分離的因素有哪些?

    尺寸排阻法的最大課題是分離條件的確立。廣泛普及的聚苯乙烯和中性糖的分離雖然可以使用公示的方法實(shí)施,但是分析各種樣品時(shí),很難得到重現(xiàn)性高的數(shù)據(jù)。影響尺寸排阻色譜法分離的因素有以下幾點(diǎn):1、離子性聚合物分析時(shí)由于離子鏈的伸縮,會(huì)對(duì)洗脫體積有影響...

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